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  • tert-Butyl 2-(3-acetylamino-2-oxo-1,2-dihydro-1-pyridyl)acetate

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    Author(s)
    Karis, N David
    Loughlin, Wendy A
    Jenkins, Ian D
    Healy, Peter C
    Griffith University Author(s)
    Jenkins, Ian D.
    Healy, Peter C.
    Loughlin, Wendy A.
    Karis, David
    Year published
    2008
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    Abstract
    The title compound, C13H18N2O4, crystallizes as discrete molecules associated as N-H...O hydrogen-bonded dimers disposed about a crystallographic inversion centre. The structure is the first solid-state structure for a 3-acetylpyridone without C-4 to C-6 substituents. The amide subsituent at C-3 is coplanar with the pyridone ring, while the tert-butyl ester group is orthogonal to the pyridine ring. The amide and ester carbonyl O atoms are not involved in strong hydrogen bonding with only a number of intramolecular and intermolecular C-H...O interactions apparent in the structure.The title compound, C13H18N2O4, crystallizes as discrete molecules associated as N-H...O hydrogen-bonded dimers disposed about a crystallographic inversion centre. The structure is the first solid-state structure for a 3-acetylpyridone without C-4 to C-6 substituents. The amide subsituent at C-3 is coplanar with the pyridone ring, while the tert-butyl ester group is orthogonal to the pyridine ring. The amide and ester carbonyl O atoms are not involved in strong hydrogen bonding with only a number of intramolecular and intermolecular C-H...O interactions apparent in the structure.
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    Journal Title
    Acta Crystallographica. Section E, Structure reports online
    Volume
    64
    Issue
    12
    Publisher URI
    http://journals.iucr.org/e/journalhomepage.html
    DOI
    https://doi.org/10.1107/S1600536808039810
    Copyright Statement
    © The Author(s) 2008. For information about this journal please refer to the journal's website. All articles published in Acta Crystallographica Section E are open access and distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. See http://creativecommons.org/licenses/by/2.0/uk/legalcode
    Subject
    Chemical Sciences
    Publication URI
    http://hdl.handle.net/10072/21285
    Collection
    • Journal articles

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