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  • Stereocontrolled synthesis of (7E,9Z)-[9,10-2H]-conjugated linoleic acid

    Author(s)
    Broustal, Garance
    Loreau, Olivier
    Griffith University Author(s)
    Broustal, Garance RJ.
    Year published
    2004
    Metadata
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    Abstract
    To study the metabolism of minor conjugated linoleic acid isomers (CLAs), (7E,9Z)-[9,10-2H] CLA was prepared in three steps from a conjugated enyne precursor. In the labelling step, deuterium atoms were introduced by partial reduction of the triple bond using deuterated disiamylborane and acetic acid-d4. Deuterated (7E,9Z) CLA was obtained with high isotopic enrichment (>99%) and purity greater than 95%. Copyright 頲004 John Wiley & Sons, Ltd.To study the metabolism of minor conjugated linoleic acid isomers (CLAs), (7E,9Z)-[9,10-2H] CLA was prepared in three steps from a conjugated enyne precursor. In the labelling step, deuterium atoms were introduced by partial reduction of the triple bond using deuterated disiamylborane and acetic acid-d4. Deuterated (7E,9Z) CLA was obtained with high isotopic enrichment (>99%) and purity greater than 95%. Copyright 頲004 John Wiley & Sons, Ltd.
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    Journal Title
    Journal of Labelled Compounds and Radiopharmaceuticals
    Volume
    47
    Issue
    12
    DOI
    https://doi.org/10.1002/jlcr.876
    Subject
    Organic Chemistry
    Pharmacology and Pharmaceutical Sciences
    Publication URI
    http://hdl.handle.net/10072/27161
    Collection
    • Journal articles

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