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dc.contributor.authorGrice, Darrenen_US
dc.contributor.authorWilson, Jennyen_US
dc.contributor.editorAnthony P. Moran, Otto Holst, Patrick J. Brennan, Mark von Itzsteinen_US
dc.date.accessioned2017-05-03T11:17:19Z
dc.date.available2017-05-03T11:17:19Z
dc.date.issued2009en_US
dc.date.modified2013-11-19T04:18:37Z
dc.identifier.isbn9780123745460en_US
dc.identifier.urihttp://hdl.handle.net/10072/29481
dc.description.abstractOutlined in this chapter are strategies for the use of the analytical techniques of nuclear magnetic resonance (NMR) spectroscopy and mass spectrometry (MS) towards the elucidation of the structures of microbial wall glycans. Specifically, the determination of the structure of capsular polysaccharide, core oligosaccharide or O-antigen utilizing 1D, 1D selective and 2D homonuclear and heteronuclear NMR experiments and database resources is presented. Described is the application of high resolution magic angle spinning techniques for studying glycopolymer structures. MS sample derivatization strategies along with associated gas chromatography-mass spectrometry, sugar, linkage, and absolute configuration analyses are outlined. The use of fast atom bombardment, matrix-assisted laser desorption ionization and electrospray-mass spectrometry ionization techniques along with their associated mass analysers are presented for characterizing oligosaccharide, lipid A, lipooligosaccahride, ipopolysaccharide and capsular polysaccharide glycan structures.en_US
dc.description.peerreviewedYesen_US
dc.description.publicationstatusYesen_US
dc.languageEnglishen_US
dc.language.isoen_US
dc.publisherAcademic Pressen_US
dc.publisher.placeOxford, UKen_US
dc.publisher.urihttp://www.sciencedirect.com/science/article/pii/B9780123745460000134en_US
dc.relation.ispartofbooktitleMicrobial Glycobiology: Structures, Relevance and Applicationsen_US
dc.relation.ispartofchapter13en_US
dc.relation.ispartofstudentpublicationNen_US
dc.relation.ispartofpagefrom233en_US
dc.relation.ispartofpageto252en_US
dc.relation.ispartofeditionFirsten_US
dc.rights.retentionYen_US
dc.subject.fieldofresearchCharacterisation of Biological Macromoleculesen_US
dc.subject.fieldofresearchcode030403en_US
dc.titleAnalytical Approaches Towards the Structural Characterization of Microbial Wall Glycopolymersen_US
dc.typeBook chapteren_US
dc.type.descriptionB1 - Book Chapters (HERDC)en_US
dc.type.codeB - Book Chaptersen_US
gro.facultyOffice of the Snr Dep Vice Chancellor, Institute for Glycomicsen_US
gro.rights.copyrightSelf-archiving is not yet supported by this publisher. Please refer to the publisher's website or contact the author(s) for more information.en_US
gro.date.issued2009
gro.hasfulltextNo Full Text


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