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  • Recent advances in the application of 13c and 15N NMR spectroscopy to soil organic matter studies

    Author(s)
    Mathers, NJ
    Mao, XA
    Xu, ZH
    Saffigna, PG
    Berners-Price, SJ
    Perera, MCS
    Griffith University Author(s)
    Berners-Price, Sue J.
    Xu, Zhihong
    Year published
    2000
    Metadata
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    Abstract
    Nuclear magnetic resonance (NMR) spectroscopy has been applied to many studies in soil science, geochemistry, and environmental science. In recent years, the study of soil organic matter (SOM) using NMR techniques has progressed rapidly. NMR spectroscopy has been used to study chemical changes of SOM during decomposition, and also of soil extract fractions such as humic acid and fulvic acid. NMR spectroscopy of soils has improved rapidly in recent years with the introduction of pre-treatment and particle-size fractionation. In addition to routine liquid- and solid-state 13C NMR applications, 15N NMR spectra of natural abundant ...
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    Nuclear magnetic resonance (NMR) spectroscopy has been applied to many studies in soil science, geochemistry, and environmental science. In recent years, the study of soil organic matter (SOM) using NMR techniques has progressed rapidly. NMR spectroscopy has been used to study chemical changes of SOM during decomposition, and also of soil extract fractions such as humic acid and fulvic acid. NMR spectroscopy of soils has improved rapidly in recent years with the introduction of pre-treatment and particle-size fractionation. In addition to routine liquid- and solid-state 13C NMR applications, 15N NMR spectra of natural abundant samples have been reported, but 15N-enriched material is more convenient to use due to the low natural abundance of 15N. Some newly developed NMR techniques have also been utilised, such as 2-dimensional NMR spectroscopy and improved 1H NMR techniques. These are reviewed and commented on in this paper.
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    Journal Title
    Australian Journal of Soil Research
    Volume
    38
    DOI
    https://doi.org/10.1071/SR99074
    Subject
    History, heritage and archaeology
    Soil sciences
    Publication URI
    http://hdl.handle.net/10072/3209
    Collection
    • Journal articles

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