Bis(2-pyrimidinyl) disulfide dihydrate: a redetermination
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Smith, G
Sagatys, DS
Healy, PC
White, JM
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Abstract
The crystal structure of bis(2-pyrimidinyl) disulfide dihydrate, C8H6N4S2粈2O, has been redetermined using CCD diffractometer data. This has allowed for a more precise location of the water H atoms and shows the water molecules forming unusual spiral hydrogen-bonded aqua columns, as well as giving inter-column crosslinks through the pyrimidine N-atom acceptors of the disulfide molecules. The structural chemistry of aromatic disulfides has also been reviewed.
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Acta Crystallographica. Section E: Structure reports online
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E60
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12
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© The Author(s) 2004. For information about this journal please refer to the journal's website. All articles published in Acta Crystallographica Section E are open access and distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. See http://creativecommons.org/licenses/by/2.0/uk/legalcode
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History, heritage and archaeology