An Efficient and Solvent-Free Synthesis of Mixed Ortho Esters

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L. Cosgrove, Kelly
P. McGeary, Ross
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2008
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Abstract

Primary, secondary and electron-deficient tertiary alcohols react rapidly with ketene dimethyl acetal to form mixed ortho esters, without catalysts and under solvent-free conditions. 1,2-Diols yield bis(mixed ortho esters), rather than cyclic ortho esters.

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Synlett

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2008

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16

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Organic Chemical Synthesis

Medicinal and Biomolecular Chemistry

Organic Chemistry

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