A reliable synthesis of 2- and 6-amino-β-cyclodextrin and permethylated-β-cyclodextrin
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Author(s)
Muderawan, IW
Ong, TT
Teck, CL
Young, DJ
Chi, BC
Ng, SC
Ong, TT
Teck, CL
Young, DJ
Chi, BC
Ng, SC
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Date
2005
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Abstract
A new, reliable method for the introduction of an amine group at positions 2 or 6 of ߭cyclodextrin and permethyl-߭cyclodextrin is described. It involves selective tosylation followed by azide substitution and almost quantitative reduction with triphenylphosphine followed by hydrolysis of the phosphinimine intermediate.
Journal Title
Tetrahedron Letters
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46
Issue
46
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© 2005 Elsevier : Reproduced in accordance with the copyright policy of the publisher : This journal is available online - use hypertext links.
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Subject
Medicinal and biomolecular chemistry
Organic chemistry