Transmission electron microscopy characterization of NaAlH4
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Author(s)
Vullum, P.
Pitt, M
Walmsley, J.
Hauback, B.
Holmestad, R.
Pitt, M
Walmsley, J.
Hauback, B.
Holmestad, R.
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2008
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Abstract
Transmission electron microscopy (TEM) has been used to characterize NaAlH4, doped with Ti, after H cycling. NaAlH4 was shown to be highly unstable under the electron beam, and "knock on" damage lead to a decomposition of NaAlH4 with Na and H evaporating from the sample. All Ti containing phases were stable under the electron beam. After H cycling, the Ti was present as a mixture of amorphous and crystalline Al1-xTix.
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Journal of Physics: Conference Series
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126
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Surfaces and Structural Properties of Condensed Matter
Atomic, Molecular, Nuclear, Particle and Plasma Physics
Condensed Matter Physics
Other Physical Sciences